Parr-instrument 6200 Manuel d'utilisateur

585M6200Isoperibol CalorimeterOperating Instruction ManualFor models produced after October 2010

1Concept of OperationParr Instrument Company8Full Microprocessor Based Process ControlThe microprocessor controller in this calorimeter has been pre-p

Installation62002www.parrinst.com9chaPter 2InstallationNote: Some of the following manual sec-tions contain information in the form of warnings, caut

2InstallationParr Instrument Company10All connections should be checked for leaks. Any leaks detected must be corrected before proceeding. Instruction

Installation62002www.parrinst.com11Swagelok Tube FittingsWhen Swagelok Tube Fittings are used, the instruc-tions for installation are:1. Simply inse

2InstallationParr Instrument Company12Figure 2-26200 Calorimeter Back Panel

Installation62002www.parrinst.com13Figure 2-3Closed Loop Configuration with 6510O2 RegulatorLine 36510 WaterHandlingSystemLine 1~27 °CLine 2Figure 2-4O

2InstallationParr Instrument Company14Figure 2-5Open Loop Configuration with 1552O2 RegulatorLine 3Tap Water· >27 °CLine 1~27 °CLine 21552WaterCoole

Instrument Description62003www.parrinst.com15chaPter 3Instrument DescriptionTypes of ControlsAll calorimeter configurations and operations are handled

Parr Instrument Company16 Notes

Program Installation & Control62004www.parrinst.com17chaPter 4Program Installation & ControlSoftware InstallationThe program in the 6200 Calor

4Program Installation & ControlParr Instrument Company18Table 4-16200 Factory Default SettingsCalorimeter OperationsOperating Mode DeterminationBo

Program Installation & Control62004www.parrinst.com19Calculation FactorsNitric Acid Factor 1.58Acid Multiplier 0.0709Sulfur Value is Percent ONSul

Parr Instrument Company20 Notes

Operating Instructions62005www.parrinst.com21chaPter 5Operating InstructionsOperating the 1108P Oxygen Combustion VesselDetailed instructions for prep

5Operating InstructionsParr Instrument Company22To speed and simplify the bucket filling process, and to conserve water and energy, Parr offers a close

Operating Instructions62005www.parrinst.com23Samples and Sample HoldersParticle Size and Moisture Content. Solid samples burn best in an oxygen bomb w

5Operating InstructionsParr Instrument Company24Foodstuffs and Cellulosic MaterialsFibrous and fluffy materials generally require one of three modes of

Operating Instructions62005www.parrinst.com25Figure 5-7 Combustion Capsule with Adhesive Tape SealUse the following procedure when filling and han-dlin

Parr Instrument Company26 Notes

Corrections & Final Reports62006www.parrinst.com27chaPter 6Corrections & Final ReportsEntering Corrections and Obtaining the Final Report Fina

www.parrinst.comTable of Contents62001Preface 4Scope 4Related Instructions 4Purpose 4Customer Service 4Explanation of Symbols 5Safety Informatio

Parr Instrument Company28 Notes

Reporting Instructions62007www.parrinst.com29chaPter 7Reporting InstructionsReport Option SectionThe 6200 Calorimeter can transmit its stored test dat

Parr Instrument Company30 Notes

File Management62008www.parrinst.com31chaPter 8File ManagementThe 6200 Calorimeter will hold data for 1000 tests in its memory. These tests may be pre

Parr Instrument Company32 Notes

Maintenance & Troubleshooting62009www.parrinst.com33chaPter 9Maintenance & TroubleshootingOxygen BombUnder normal usage the 1108P Parr Oxygen

9Maintenance & TroubleshootingParr Instrument Company34before the Start button lights up. This is to make sure that all of the jacket water is st

Menu Operating Instructions6200Awww.parrinst.com35aPPendix a Menu Operating Instructions The settings and controls are organized into ten main sectio

AMenu Operating InstructionsParr Instrument Company36Temperature Plot SetupEnable Bucket: Toggles ON/OFF.Bucket Autoscale: Toggles ON/OFF.Enable Jac

Menu Operating Instructions6200Awww.parrinst.com37Operating Controls MenuMethod of Operation: Offers an operating mode of either dynamic or equilibri

Parr Instrument CompanyTable of Contents2Chapter 8 31File Management 31Clearing Memory 31Removable SD Memory 31Chapter 9 33Maintenance & Troub

AMenu Operating InstructionsParr Instrument Company38Program Information and Control MenuDate & Time Settings: Access the sub-menu on which Date

Menu Operating Instructions6200Awww.parrinst.com39Compare Settings With Factory Defaults: This button will bring up a screen that will show the diffe

AMenu Operating InstructionsParr Instrument Company40Bomb 1EE Value: Displays the calculated EE value for the corresponding Bomb 1. Number of Runs:

Menu Operating Instructions6200Awww.parrinst.com41Manual EE Entry: This key allows the user to manually enter an EE or calibration factor for a given

AMenu Operating InstructionsParr Instrument Company42Determination CorrectionFixed Fuse Correction: Displays both the ON/OFF of the fixed fuse correct

Menu Operating Instructions6200Awww.parrinst.com43Use Offset Correction (ISO): The thermochemi-cal calculations used for treatment of nitric acid and

AMenu Operating InstructionsParr Instrument Company44Automatic Sample ID ControlsAutomatic Sample ID: When set to ON it will automatically assign sam

Menu Operating Instructions6200Awww.parrinst.com45Reporting Controls MenuReport Width: The column width of the printer being used can be set to 40 or

AMenu Operating InstructionsParr Instrument Company46Balance Port CommunicationsCustomize Balance Settings: Accesses sub-menu that sets the communica

Menu Operating Instructions6200Awww.parrinst.com47File ManagementRun Data File Manager: This key activates the File Manager. The File Manager is used

www.parrinst.comTable of Contents62003Tables Table 4-1 6200 Factory Default Settings 18Table B-1 Settings for ISO & BSI Methods 52Tabl

AMenu Operating InstructionsParr Instrument Company48Diagnostics MenuAllows the user to test many of the components and subsystems of the calorimeter.

Calculations6200Bwww.parrinst.com49aPPendix BCalculationsCalculating the Heat of CombustionThe 6200 Calorimeter will automatically make all of the cal

BCalculationsParr Instrument Company50Users may find it convenient to enter a fixed value for the fuse correction and avoid the need to determine this c

Calculations6200Bwww.parrinst.com51Thermochemical Calculation DetailsTraditionally, standard solutions and procedures have been established to simplif

BCalculationsParr Instrument Company52Using the default acid and sulfur multipliers as well as a heat of formation of nitric acid of 14.1 cal/milli-eq

Calculations6200Bwww.parrinst.com53ASTM Treatment for Acid and SulfurIn the ASTM treatment, the correction for acid formation assumes that all the aci

BCalculationsParr Instrument Company54Spiking SamplesIt is sometimes necessary to add a spiking material to samples which are very small, have a low h

Standardization6200Cwww.parrinst.com55aPPendix cStandardizationStandardizing the CalorimeterThe Energy Equivalent FactorThe term “standardization”, as

CStandardizationParr Instrument Company56Any outliers or other tests which should not be included in the average EE Value must be deleted from the mem

Standardization6200Cwww.parrinst.com57Table C-2 Calorimeter Control Limit Values in cal/g When Benzoic Acid is Used as a Test SampleAccepted heat of c

PrefaceParr Instrument Company4Preface ScopeThis manual contains instructions for installing and operating the Parr 6200 Calorimeter. For ease of use,

CStandardizationParr Instrument Company58Table C-3Calorimeter Control Limit Values in BTU/lb When Benzoic Acid is Used as a Test SampleAccepted heat o

Communications Interfaces6200Dwww.parrinst.com59aPPendix dCommunications Interfaces Printer PortUSB ConnectionThe 6200 Calorimeter is also equipped wi

DCommunications InterfacesParr Instrument Company60Generic InterfaceField Lengthdata 9CR 1The data field should consist of 9 numeric charac-ters (0 thr

Communications Interfaces6200Dwww.parrinst.com61Ethernet InterfaceCalorimeter test data can be transferred to an Eth-ernet network connected computer

DCommunications InterfacesParr Instrument Company62Samba Server Feature (Optional)Samba was originally developed as an implementa-tion of the SMB (Ser

Communications Interfaces6200Dwww.parrinst.com63The following screenshot illustrates the contents of the calorimeter data directory as presented by a

DCommunications InterfacesParr Instrument Company64The calorimeter offers a web server service. Test reports can be viewed with a web browser using a

Communications Interfaces6200Dwww.parrinst.com65Clicking on the Config button will display the screen below. Changes made on this screen will change th

DCommunications InterfacesParr Instrument Company66Clicking on the Run Data button displays a list of reports currently in the instrument memory.Click

Communications Interfaces6200Dwww.parrinst.com67Clicking on the System Info button will display the screen below.

Preface6200www.parrinst.com5Safety InformationTo avoid electrical shock, always:1. Use a properly grounded electrical outlet of correct voltage and c

DCommunications InterfacesParr Instrument Company68Clicking on the LCD Snap Shot button will display the current menu screen displayed by the calorime

Communications Interfaces6200Dwww.parrinst.com69Clicking on the Documentation button will display the screen below. Clicking on any of the links will

DCommunications InterfacesParr Instrument Company70Bar Code PortThe use of barcodes in the laboratory has become a highly accurate, rapid and inexpens

Technical Service6200Ewww.parrinst.com71aPPendix eTechnical Service Should you need assistance in the operation or ser-vice of your instrument, please

Parr Instrument Company72 Notes

Parts Lists & Drawings6200Fwww.parrinst.com73aPPendix fParts Lists & DrawingsPrincipal Assemblies in CalorimeterItem Description1108P Oxygen C

FParts Lists & DrawingsParr Instrument Company74Parts List for A1284DD2 Stirrer Hub AssemblyItem Description1282DD Hub, Stirrer1283DD2 Shaft, Stir

Parts Lists & Drawings6200Fwww.parrinst.com75Figure F-16200 Isoperibol Calorimeter Cutaway Front

FParts Lists & DrawingsParr Instrument Company76Figure F-26200 Isoperibol Calorimeter Cutaway Rear

Parts Lists & Drawings6200Fwww.parrinst.com77Figure F-3A1279DD2 Control SchematicJ10P6P8USB PORTJ8J1CONNECTS IN UPPER PORTBACK PANELUSB PORTPIN #1

PrefaceParr Instrument Company6Frequency: Calorimeters can be operated from either a 50 or 60 Hertz power supply without affect-ing their operation or

FParts Lists & DrawingsParr Instrument Company78Figure F-4Oxygen Solenoid Assembly & Fittings

Parts Lists & Drawings6200Fwww.parrinst.com79Figure F-5Water Tank Assembly

FParts Lists & DrawingsParr Instrument Company80Figure F-6A1311DD Circulating Pump Assembly

Parts Lists & Drawings6200Fwww.parrinst.com81Figure F-7Temperature Control Assembly with Fittings

FParts Lists & DrawingsParr Instrument Company82Figure F-8A1284DD2 Stirrer Hub Assembly

Parts Lists & Drawings6200Fwww.parrinst.com83Figure F-9Stirrer Motor Assembly

Parr Instrument Company84 Notes

585M R04 09/11/14

Concept of Operation62001www.parrinst.com7chaPter 1Concept of OperationOverview• The 6200 Calorimeter has been designed to provide the user with:• A