Parr-instrument Series 4540 Manuel d'utilisateur télécharger pdf (Page 2)

4540 High Pressure Reactor System

Parr Instrument Company

PREFACE 3

Scope 3

Related Instructions 3

Intended Usage 3

Safety Information 3

General Speciﬁcations 3

Explanation of Symbols 4

Environmental Conditions 4

Unpack Carefully 4

Provisions for Lifting and Carrying 4

Cleaning & Maintenance 4

User’s Responsibility 5

FIXED HEAD OR REMOVABLE HEAD DESIGN 6

Vessel Head Design 6

PTFE Flat Gasket 6

INSTALLATION 7

Pressure and Temperature Limits 7

Assemble the Reactor 8

IDENTIFY THE VALVES 9

Gas Inlet Valves 9

Gas Release Valve 9

Liquid Sampling Valve 9

OTHER VESSEL HEAD FITTINGS 10

Safety Rupture Disc 10

Type J Thermocouple 10

Pressure Gage 10

Gage and Valve Adapters 10

ACCESSORIES 11

Serpentine Cooling Coil 11

Spare Parts Kit 11

Liners 11

Variable Speed Electric Motor 11

Air Motor 11

Pneumatic Lift for Fixed Head Vessels 12

HOW TO USE THE VESSEL 13

Fixed Head Vessels 13

Removable Head Vessels 13

MAINTENANCE 15

General Maintenance Notes 15

Periodic Pressure Tests 16

Technical Support 16

4540 SERIES REACTION VESSEL PARTS LIST 17

Standard Vessel Fittings 17

Heaters Parts List 19

Overarm Parts List 20

4540 SERIES DRAWINGS 22

4540 Series Vessel with Fittings 22

1/4 HP Light Duty FH/RH Overarm and Motor 24

1/8 HP Light Duty FH/RH Vessel Overarm and Motor 25

4544 600 mL Removable Head Reactor 26

4545 600 mL Fixed Head Reactor 27

4544/4544A 600 mL Removable Head Reactor 28

4545/4545A 600 mL Fixed Head Reactor 29

4546 1200 mL Removable Head Reactor 30

4547 1200 mL Fixed Head Reactor 31

Customer Service

Questions concerning the installation or operation

of this instrument can be answered by the Parr

Customer Service Department:

1-309-762-7716 • 1-800-872-7720

Fax: 1-309-762-9453

E-mail: [email protected]

www.parrinst.com

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Parr-instrument Series 4540 Manuel d'utilisateur Page 2

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