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6725 Semi-micro Calorimeter Instruction Manual
1-1
PREFACE
Scope
This manual contains instructions for installing and operating the Parr 6725 Semi-micro
Calorimeter. For ease of use, the manual is divided into 13 chapters.
Installation
Quick Start
Operation
Menu Descriptions
Calculations
Reports
Memory Management
Maintenance
Troubleshooting
Technical Service
Parts Lists
Drawings
Tables
Subsections of these chapters are identified in the Table of Contents.
To assure successful installation and operation, the user must study all instructions
carefully before starting to use the 6725 Semi-micro Calorimeter to obtain an
understanding of the capabilities of the equipment and the safety precautions to be
observed in the operation.
Additional instructions concerning the installation and operation of various component
parts and peripheral items used with the 6725 Semi-micro Calorimeter should be made a
part of these instructions. Additional instructions for the optional printer are found in the
respective printer package and should be made a part of this book.
No. Description
201M Limited Warranty
492M Operating Instructions for the 1109A Semi-micro Oxygen Bombs
207M Analytical Methods for Oxygen Bombs
230M Safety in the Operation of Laboratory and Pressure Vessels
483M Introduction to Bomb Calorimetry
This manual contains detailed instructions related to oxygen bomb calorimetry,
standardization of the calorimeter, combustion techniques, and thermochemical
corrections.
Note:
The unit of heat used in this manual is the International Table
(IT) calorie, which is equal to 4.1868 absolute joules.
- TABLE OF CONTENTS 2
- PREFACE 4
- Explanation of Symbols 5
- Safety Information 5
- INSTALLATION 7
- Communication Connections 9
- Printer Connections 9
- Balance Connections 9
- Bar Code Port 11
- Computer Connections 11
- QUICK START 19
- OPERATION 21
- Performing an analysis 23
- MENU DESCRIPTIONS 28
- Temperature vs. Time Plot 29
- Temperature Plot Setup Menu 29
- Operating Controls Menu 30
- Spike Controls 31
- Standardization Correction 37
- Determination Correction 38
- Calculation Factors Menu 39
- Net Heat/Dry Heat Factors 40
- Data Entry Controls Menu 40
- Reporting Controls Menu 42
- Communication Controls Menu 43
- File Management Menu 44
- Run Data File Manager 45
- Diagnostics Menu 46
- CALCULATIONS 49
- Manual vs. Fixed Corrections 50
- Definitions 51
- ASTM, ISO and Other Methods 55
- REPORTS 57
- MEMORY MANAGEMENT 59
- MAINTENANCE 60
- TROUBLESHOOTING 61
- TECHNICAL SERVICE 63
- PARTS LISTS 64
- DRAWINGS 66
- 493E Plug 69
- Table 1 – Default Settings 73
- Table 1 – Continued 74
- Value -43.5 75
- Revision 03/15/11 76
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