Parr-instrument Series 4590 Manuel d'utilisateur télécharger pdf (Page 3)

4590 Micro Reactors

www.parrinst.com

3

PREFACE 4

Scope 4

Related Instructions 4

Intended Usage 4

Safety Information 4

General Speciﬁcations 4

Electrical Ratings 4

Explanation of Symbols 5

Environmental Conditions 5

Unpack Carefully 5

Provisions for Lifting and Carrying 5

Cleaning & Maintenance 5

User’s Responsibility 6

Fixed Head or Removable Head Vessel Design 7

Flat Gasket or Self Sealing O-Ring Closure 7

INSTALLATION 8

Pressure and Temperature Limits 8

Assemble The Reactor 9

IDENTIFY THE VALVES 10

Gas Inlet Valve 10

Gas Release Valve 10

Liquid Sampling Valve 10

OTHER VESSEL HEAD FITTINGS 11

Safety Rupture Disc 11

Type J Thermocouple 11

Pressure Gage 11

ACCESSORIES AND OPTIONS 11

Liners 11

Spare Parts Kit 11

Air Motor 12

HOW TO USE THE VESSEL 14

To open the Vessel 14

Before Closing the Vessel 14

Sealing Vessels with PTFE Gaskets 14

Sealing with Flexible Graphite Gaskets 14

O-Ring Closures 14

Gas Connections 15

Pressurizing the Vessel 15

Do Not Overﬁll the Vessel 15

Releasing Pressure 15

Withdrawing Liquid Samples 15

Initial Operating Test 15

MAINTENANCE 16

General Maintenance Notes 16

Periodic Pressure Tests 17

Technical Support 17

SERIES 4590 VESSEL PARTS LISTS 18

Standard Reaction Vessel Parts List 18

High Pressure Reaction Vessel Parts List 21

HP/HT Reaction Vessel Parts List 23

Overarm and Stand Parts List 24

Support Stands 25

Customer Service

Questions concerning the installation or operation

of this instrument can be answered by the Parr

Customer Service Department:

1-309-762-7716 • 1-800-872-7720

Fax: 1-309-762-9453

E-mail: [email protected]

http://www.parrinst.com

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