Parr-instrument Series 4540 Manuel d'utilisateur

394M4540High Pressure ReactorsOperating Instruction Manual

4540 High Pressure Reactor SystemParr Instrument Company10PRESSURE GAGE209HC4208HC1556HCPHA455VB21446HC491HCADA451VB208HC6209HC4INLET SAMPLING VALVE20

4540 High Pressure Reactor Systemwww.parrinst.com11ACCESSORIES Serpentine Cooling CoilA Serpentine Cooling Coil can be installed in any of these react

4540 High Pressure Reactor SystemParr Instrument Company12Pneumatic Lift for Fixed Head VesselsHand Lever Valve Assembly “Joystick”Lift up on joystic

4540 High Pressure Reactor Systemwww.parrinst.com13HOW TO USE THE VESSELFixed Head VesselsFirst, lower the heater and push it aside before at-temptin

4540 High Pressure Reactor SystemParr Instrument Company14Gas ConnectionsGas connections are dependent on applications. For general usage, use the pre

4540 High Pressure Reactor Systemwww.parrinst.com15MAINTENANCEGeneral Maintenance Notes1. Periodically inspect all electrical wiring and pres-sure co

4540 High Pressure Reactor SystemParr Instrument Company16Periodic Pressure TestsEach cylinder used in a Parr stirred reactor is tested under hydrost

4540 High Pressure Reactor Systemwww.parrinst.com174540 SERIES REACTION VESSEL PARTS LISTStandard Vessel Fittings(5000 psig/ 350 °C)Consult the itemiz

4540 High Pressure Reactor SystemParr Instrument Company18ShaftsPart No. Description Code352HC10 Stub Shaft, mag drive RV352HC11 Stub Shaft, mag drive

4540 High Pressure Reactor Systemwww.parrinst.com19Heaters Parts ListHeaters for Bench Top and Floor Stand VesselsPart No. DescriptionA2256HC12EBHeat

4540 High Pressure Reactor SystemParr Instrument Company2PREFACE 3Scope 3Related Instructions 3Intended Usage 3Safety Information 3General S

4540 High Pressure Reactor SystemParr Instrument Company20* For Special FittingsOverarm Parts ListMotorPart No. Description Code1355EES Motor, VS/PM 1

4540 High Pressure Reactor Systemwww.parrinst.com21OPTICAL WHEELDRIVE PULLEYMOTORENCASEMENTOVERARM PLATEISOLATORBELT GUARDSNAP RINGRELEASE KNOBHUB ASS

4540 High Pressure Reactor SystemParr Instrument Company224540 SERIES DRAWINGS4540 Series Vessel with FittingsShown with Standard Magnec Drive299HC BU

4540 High Pressure Reactor Systemwww.parrinst.com232301HC7 HEAD1133HC BUSHING (UNDERSIDE) REF2996HC COLLAR (UNDERSIDE) REFA2140HC2 MAG DRIVE REFFIXED

4540 High Pressure Reactor SystemParr Instrument Company241/4 HP Light Duty FH/RH Overarm and MotorDiagram of Overarm for: 4544A, 4545A, 4546A &

4540 High Pressure Reactor Systemwww.parrinst.com251/8 HP Light Duty FH/RH Vessel Overarm and MotorDiagram of Overarm for: 4544A, 4545A, 4546A, &

4540 High Pressure Reactor SystemParr Instrument Company264544 600 mL Removable Head ReactorWithout Bottom Drain Valve

4540 High Pressure Reactor Systemwww.parrinst.com274545 600 mL Fixed Head Reactor Without Bottom Drain Valve

4540 High Pressure Reactor SystemParr Instrument Company284544/4544A 600 mL Removable Head ReactorWith or Without Bottom Drain Valve

4540 High Pressure Reactor Systemwww.parrinst.com294545/4545A 600 mL Fixed Head ReactorWith or Without Bottom Drain Valve

4540 High Pressure Reactor Systemwww.parrinst.com3PREFACEScopeThese instructions describe the installation, opera-tion and maintenance of Parr Series

4540 High Pressure Reactor SystemParr Instrument Company304546 1200 mL Removable Head ReactorWithout Bottom Drain Valve

4540 High Pressure Reactor Systemwww.parrinst.com314547 1200 mL Fixed Head ReactorWithout Bottom Drain Valve

394M R02 12/30/14

4540 High Pressure Reactor SystemParr Instrument Company4Explanation of SymbolsII On position, full power heater switchI On position, half power heate

4540 High Pressure Reactor Systemwww.parrinst.com5User’s ResponsibilityAll Parr reactors and pressure vessels are designed and manufactured with great

4540 High Pressure Reactor SystemParr Instrument Company6FIXED HEAD OR REMOVABLE HEAD DESIGNParr Series 4540 High Pressure Reactors are furnished with

4540 High Pressure Reactor Systemwww.parrinst.com7INSTALLATIONPressure and Temperature LimitsThe working pressure and temperature at which any reactor

4540 High Pressure Reactor SystemParr Instrument Company8Assemble the ReactorThese reactors require at least 10 square feet of work-space in a well-ve

4540 High Pressure Reactor Systemwww.parrinst.com9IDENTIFY THE VALVES Gas Inlet ValvesThe gas inlet valve is easily identified when the bomb is open by